Details
Excellent chemical plant bulk supply tetramisole 5036-02-2
- Molecular Formula: C11H12N2S
- Molecular Weight: 204.296
- Appearance/Colour: white to off-white crystalline powder
- Melting Point: 87-89°
- Boiling Point: 344.4 °C at 760 mmHg
- PKA: 10.00±0.40(Predicted)
- Flash Point: 162.1 °C
- PSA： 40.90000
- Density: 1.32 g/cm3
- LogP: 2.32160
tetramisole(Cas 5036-02-2) Usage
InChI:InChI=1/C11H12N2S/c1-2-4-9(5-3-1)10-8-13-6-7-14-11(13)12-10/h1-5,10H,6-8H2
5036-02-2 Relevant articles
Preparation method of tetraimidazole hydrochloride
-
Paragraph 0026-0044, (2021/02/13)
The invention provides a preparation met...
Preparation method of tetraimidazole free alkali
-
Paragraph 0011; 0033-0058, (2020/07/24)
The invention discloses a preparation me...
Total Synthesis of (+)-Granatumine A and Related Bislactone Limonoid Alkaloids via a Pyran to Pyridine Interconversion
Schuppe, Alexander W.,Zhao, Yizhou,Liu, Yannan,Newhouse, Timothy R.
supporting information, p. 9191 - 9196 (2019/06/17)
We report the first total synthesis of (...
DIHYDRO-5,6 IMIDAZOTHIAZOLES, DIHYDRO-2,3 IMIDAZOBENZOTHIAZOLES, ANALOGUES DU LEVAMISOLE
Amarouch, H.,Loiseau, P. R.,Bonnafous, M.,Caujolle, R.,Payard, M.,et al.
, p. 421 - 438 (2007/10/02)
New compounds containing 5,6-dihydro imi...
5036-02-2 Process route
-
-
N-(2-chloroethyl)-α-(chloromethyl)benzylamine hydrochloride
-
-
17356-08-0
thiourea
-
-
5036-02-2
Tetramisole
| Conditions | Yield |
|---|---|
|
With
sodium hydroxide;
In
aq. buffer;
at 80 - 85 ℃;
for 5.5h;
pH=9;
pH-value;
|
91.58%
|
-
-
3882-98-2
2-amino-4,5-dihydrothiazole hydrochloride
-
-
102921-26-6,93-52-7
(1,2-dibromoethyl)benzene
-
-
5036-02-2
Tetramisole
| Conditions | Yield |
|---|---|
|
2-amino-4,5-dihydrothiazole hydrochloride; (1,2-dibromoethyl)benzene;
With
sodium carbonate;
In
N,N-dimethyl-formamide;
at 85 ℃;
for 2h;
In
N,N-dimethyl-formamide;
at 160 ℃;
for 16h;
Temperature;
Reagent/catalyst;
|
87.54%
|
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5036-02-2 Downstream products
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65172-59-0
1,3-bis-(4-chloro-phenyl)-6-phenyl-tetrahydro-thiazolo[2',3':2,3]imidazo[1,2-a ][1,3,5]triazine-2,4-dione
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65172-56-7
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65172-58-9
1,3,6-triphenyl-tetrahydro-thiazolo[2',3':2,3]imidazo[1,2-a ][1,3,5]triazine-2,4-dione
-
65172-53-4
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